SPM Application in Polymer Material SII( eiko Instruments Inc Phase Separation Structure Lamella Structure ABS resin LD, MD, HD- Polyethylene PC/AES alloy Linear Ld Polyethylene PC/ABS alloy UH Molecular Weight PE ABS/PVC alloy Polypropylene etc etc Micro Pss Next generation Thermoplastic Elastomer Conducting Polymer Styrene butadiene- Organic el Polyester- Biodegradable Polymer Polyvinyl Chloride- etc
Phase Separation Structure ・ABS resin ・PC/AES alloy ・PC/ABS alloy ・ABS/PVC alloy etc Lamella Structure ・LD-, MD-, HD- Polyethylene ・Linear LD Polyethylene ・UH Molecular Weight PE ・Polypropylene etc Next Generation ・Conducting Polymer ・Organic EL ・Biodegradable Polymer etc Micro PSS Thermoplastic Elastomer ・Styrene Butadiene- ・Polyester- ・Polyvinyl Chlorideetc SPM Application in Polymer Material
Structure and Function of polymer Morphology observation with SPM SII C eiko Instruments Inc OBservation in the heating process with the air OSurface and Interface Information Observation in the inert gas ODifficult sample for TEM(Rubber/Rubber blend) Structure Function Heating/Cooling S PM
Structure Function Heating/Cooling ＳＰＭ ●Observation in the heating process with the air ●Surface and Interface Information ●Observation in the inert gas ●Difficult sample for TEM（Rubber/Rubber blend） Structure and Function of Polymer ー Morphology observation with SPM ー
Material Characterization using SPM SII O eiko Instruments Inc Visco-elasticity VE-AFMDFM Phase Friction force Polymer characterization in PM nano scale level (FFM/LM-FEM Hardness Adhesive Force adhesio Glass trans
Visco-elasticity Friction Force Adhesive Force Glass trans. Phase Hardness Polymer characterization in nano scale level VE-AFM/DFM PM FFM/LM-FFM Adhesion Material Characterization using SPM
Material Characterization DFM/PM (Phase mode) measurement SII C Seiko Instruments Inc 【 Purpose Distribution of the characteristics change in the polymer surface can e observed ( Principle Detecting the phase change in DFM measurement 【 Advantage Simultaneous imaging with DFM 2 Same advantage as DFM for the soft or charged surface (which is difficult to apply lM-FFM or VE-AFM) Topography(7um) resin Observed image of the heat shrinkage rubber silicon (resin/silicon rubber) rubber
【Purpose】 ◆ Distribution of the characteristics change in the polymer surface can be observed. 【Principle】 ◆Detecting the phase change in DFM measurement 【Advantage】 ◆Simultaneous imaging with DFM ◆Same advantage as DFM for the soft or charged surface. (which is difficult to apply LM-FFM or VE-AFM) resin silicon rubber Topography（７μｍ） PM image（７μｍ） Material Characterization DFM／PM （Phase mode）measurement Observed image of the heat shrinkage rubber （resin/silicon rubber） →
Phase(PM: Phase Mode) measurement Structure and Function of polymer SII C eiko Instruments Inc (SPA-300HV, Environment Control Type Unit) Data No. 1 Lamella structure of Polypropylene Topography PM image 100nm 100nr EPR LAmella structure can be observed clearly with PM mode. O Domain of Ethylene Propylene Rubber(EPR)is distributed in the Polypropylene(PP)matrix
100 nm 100 nm Topography PM image EPR PP （matrix） ●Lamella structure can be observed clearly with PM mode. ●Domain of Ethylene Propylene Rubber (EPR) is distributed in the Polypropylene (PP) matrix. （ SPA-300HV, Environment Control Type Unit） Data No.１ Lamella structure of Polypropylene Phase（PM：Phase Mode）measurement － Structure and Function of Polymer －