《美国FDA农残分析手册》（第一卷英文版）APPENDIX I：PESTDATA

a Appendix l: PESTDATA Chemicals in Order by Chemical Name(continued) Molecular RRT/c Rrt/c rrt/c Formula OV-101 ov-225 Ov-17 03 304 Ethers CH,CL, C12H6.1013.9 0.58 0.47 4185 105 1.88 1.6 Responses: OV-101: TRoO Aroclor 1254* 107 13 1.3 182 1.17 1.84 1.48 2.68 1.6 3.14 1.75 3.7 3.3 4.8 Responses: OV-101: TR30 Aroclor 1260* C12H3.7016.3 131 1.17 61 685

Pesticide Analytical Manual Vol. I APPENDIX I Form FDA 2905a (6/92) Transmittal No. 2000-1 (10/1999) Molecular RRT/c RRT/c RRT/c Name Formula OV-101 OV-225 OV-17 302 303 304 Ethers CH2Cl2 Appendix I–11 Appendix I: PESTDATA Chemicals in Order by Chemical Name (continued) Recoveries Aroclor 1248* C12H6.1Cl3.9 0.52 0.4 - - C C 6 1 0.58 0.47 - 0.68 0.54 - 0.82 0.61 - 0.87 0.68 - 0.98 0.85 - 1.05 0.9 - 1.25 0.98 - 1.42 1.1 - 1.52 1.18 - 1.77 1.37 - 1.88 1.6 - 2.24 1.75 - 2.59 2.01 - 3.1 2.72 - Responses: OV-101: TR50 Aroclor 1254* C12H5Cl5 - - 0.35 - C C 6 1 0.89 0.68 0.48 1 0.85 0.63 1.07 0.9 0.81 1.3 0.99 0.97 1.55 1.1 1.3 1.82 1.17 1.43 1.92 1.39 1.84 2.24 1.48 1.98 2.68 1.6 2.26 3.14 1.75 2.55 3.7 2.03 2.91 4.2 2.46 3.3 4.4 2.79 4.3 5 3.8 4.8 5.9 4.3 5.2 Responses: OV-101: TR30 Aroclor 1260* C12H3.7Cl6.3 - 1.09 - - C C 6 1 1.31 1.17 - 1.53 1.61 - 1.9 1.81 - 2.11 2.06 - 2.25 2.18 - 2.68 2.45 - 2.9 2.76 -

P Appendix l: PESTDATA Chemicals in Order by Chemical Name(continued Molecular RRT/c Rrt/c rrt/c Recoveries Formula OV-101 ov-225 Ov-17 303304 3.12 3.6 3.48 5.9 7.2 Aroclor 1262* C12H3.3C16.7 6826255 9 Responses: OV-101: TR20 Aroclor 1268* CI2HICI9 7.3 Responses: OV-101: N40 Aroclor 4465* CI (MIX) 2.08 288 品二己二≤一 3.11

Pesticide Analytical Manual Vol. I APPENDIX I Transmittal No. 2000-1 (10/1999) Form FDA 2905a (6/92) Appendix I–12 Molecular RRT/c RRT/c RRT/c Name Formula OV-101 OV-225 OV-17 302 303 304 Ethers CH2 Cl2 Appendix I: PESTDATA Chemicals in Order by Chemical Name (continued) Recoveries Aroclor 1260* (cont’d) 3.2 3.12 - 3.6 3.48 - 4.2 3.7 - 5 4.3 - 5.9 5.2 - 6.6 5.8 - 8 7.2 - 9.3 8.8 - Responses: OV-101: TR20 Aroclor 1262* C12H3.3Cl6.7 1.29 - - - C C 6 1 1.53 - - 1.89 - - 2.11 - - 2.26 - - 2.66 - - 2.88 - - 3.12 - - 3.6 - - 4.2 - - 5 -- 5.9 - - 6.5 - - 6.7 - - 8 -- 9.3 - - Responses: OV-101: TR20 Aroclor 1268* C12H1Cl9 3.8 - - - C - 6 - 4.7 - - 5.4 - - 7.3 - - 8.7 - - 10 - - 13 - - 16.2 - - Responses: OV-101: NI40 Aroclor 4465* CHCl (MIX) 2.08 - - - C C 6 1 2.22 - - 2.67 - - 2.88 - - 3.11 - -

a Appendix l: PESTDATA Chemicals in Order by Chemical Name(continued) Molecular RRT/c Rrt/c rrt/c Formula OV-101 ov-225 Ov-17 303 304 Ethers CH Cl, 9 6.5 OV-101: TR4 atrazine C8HI4CIN3 0.74 44 Responses: OV-101: TL8/TR200 OV-17: NI20 azafenidin CI5HISCI2N302 Responses: OV-101:NI(WB)90 hos-ethyl CI2HI6N303PS2 14.8 Responses: OV-101: T158/TR200 OV-17: FP(WB)26/N120 CIOH12N3O3PS2 l1.8 C 6-15501-23 Responses: OV-101: T130/TR5O azinphos-methyl oxygen analog CIOHI2N304PS Responses: OV-101: FP20 OV-17: FP(WB)42 C9H6O3SNC bendiocarb ClIHI3NO4 Responses: DEGS: NPI benfluralin CI3H16F3N30 0.18 HX(B)15/N(WB)2 OV-17: HX(WB)I OV-225: NI2 CIsHIOINO 2.43 Responses: OV-101: NP60 benoxacor CllHIICI2NO2 0.64 0.7 15+50 Responses: OV-101: NIl/NP6 OV-17: NII/NP7 OV-225: NI2 bensulide 20.2 sponses: OV-101: FP100/N(WB)9/T90 OV-17: FP100

Pesticide Analytical Manual Vol. I APPENDIX I Form FDA 2905a (6/92) Transmittal No. 2000-1 (10/1999) Molecular RRT/c RRT/c RRT/c Name Formula OV-101 OV-225 OV-17 302 303 304 Ethers CH2Cl2 Appendix I–13 Appendix I: PESTDATA Chemicals in Order by Chemical Name (continued) Recoveries Aroclor 4465* (cont’d) 3.6 - - 4.2 - - 4.5 - - 5 -- 5.4 - - 5.9 - - 6.5 - - 6.6 - - 8 -- 9.3 - - 12.1 - - Responses: OV-101: TR40 atrazine C8H14ClN5 0.43 0.74 0.44 C S # NR 50 1-2-3 Responses: OV-101: TI58/TR200 OV-17: NI20 azafenidin C15H13Cl2N3O2 14 - - V - - - - Responses: OV-101:NI(WB)90 azinphos-ethyl C12H16N3O3PS2 6.9 - 14.8 C P S 50 3 Responses: OV-101: TI58/TR200 OV-17: FP(WB)26/NI20 azinphos-methyl C10H12N3O3PS2 5.2 - 11.8 C NR NR 6-15-50 1-2-3 Responses: OV-101: TI30/TR50 azinphos-methyl oxygen analog C10H12N3O4PS 3.7 - 10.1 C - - - - Responses: OV-101: FP20 OV-17: FP(WB)42 benazolin methyl ester C9H6O3SNCl 0.99 - - - - - - - Responses: OV-101: NI1 bendiocarb C11H13NO4 0.32 - - C - - - - Responses: DEGS: NP13 benfluralin C13H16F3N3O4 0.37 0.28 0.18 C C C 6 2 Responses: OV-101: HX(WB)1.5/NI(WB)2 OV-17: HX(WB)1 OV-225: NI2 benodanil C13H10INO 2.43 - 4.5 C - - - - Responses: OV-101: NP60 benoxacor C11H11Cl2NO2 0.64 1.06 0.7 C P C 15+50 2+3 Responses: OV-101: NI1/NP6 OV-17: NI1/NP7 OV-225: NI2 bensulide C14H24NO4PS3 9.5 - 20.2 C P C 50 3 Responses: OV-101: FP100/NI(WB)9/TI190 OV-17: FP100

P Appendix l: PESTDATA Chemicals in Order by Chemical Name(continued Molecular RRT/c Rrt/c rrt/c Formula OV-101 ov-225 Ov-17 3304 CI8HI7CI2NO3 615-501-23 Responses: OV-101: NI(WB)3 OV-17: NIS OV-225: NI6 6H6C16 BHC, beta- C6H6CI 0.43 0.56 Responses: OV-101: TR2 OV-17: NIl BHC, delta- C6H6C16 0.5 1.71 0.67 Responses: OV-101: FXO.5/TRO. 4 OV-17: N10.5 149 C 15+502+3 OV-101: HX16/NI4 bifenthrin C23H22CIF902 Responses: OV-101: NI8 OV-17: HX5/HX(WB)20 Cl5HISN206 Responses: OV-101: NI(WB)I OV-17: N22/NP(WB)I0 bis(2-ethylhexyl) phthalate C24H38O4 15+50 Responses: OV-101: NI(V)200 bis(trichloromethyl)disulfide C2C16s2 bitertanol C20H23N3O2 9.4 12.5 C9HISBrN202 C 615501-23 Responses: OV-101: HN(WB)2/NI(WB)2/NP(WB)I7 OV-17: HN(WB)I/HX(WB)8/NI(WB)6/NP(WB)5 OV-225: NI(WB)12 bromacil methyl ether CIoHI6BrN20 HN(WB)1.2/HX(WB)90/NI(WB)1.5/NP(WB)10 OV-225: NI(WB)3.8 HI bromofenoxim methyl ether Cl4H9Br206N3 Responses: OV-101: HN(WB)6/NI1 CSHSBrCI2O3PS 1.16 Responses: OV-101: FP3/NI(WB)1/T13 OV-17: FP3/NI2 OV-225: NI6 CIoH12BrCI203PS Responses: OV-101: FP3/N13/TI4 OV-17: FP(WB)0.3 CI7H16Br203 C群 15+50 1-23 Responses: OV-101: TRI2 品二己二≤一

Pesticide Analytical Manual Vol. I APPENDIX I Transmittal No. 2000-1 (10/1999) Form FDA 2905a (6/92) Appendix I–14 Molecular RRT/c RRT/c RRT/c Name Formula OV-101 OV-225 OV-17 302 303 304 Ethers CH2 Cl2 Appendix I: PESTDATA Chemicals in Order by Chemical Name (continued) Recoveries benzoylprop-ethyl C18H17Cl2NO3 4.3 8.4 6 P NR NR 6-15-50 1-2-3 Responses: OV-101: NI(WB)3 OV-17: NI8 OV-225: NI6 BHC, alpha- C6H6Cl6 0.4 0.48 0.35 C C C 6 1 Responses: OV-101: TR0.4 OV-17: NI0.3 BHC, beta- C6H6Cl6 0.43 1.62 0.56 C C C 6 1 Responses: OV-101: TR2 OV-17: NI1 BHC, delta- C6H6Cl6 0.5 1.71 0.67 C C C 6+15 1 Responses: OV-101: HX0.5/TR0.4 OV-17: NI0.5 bifenox C12H9Cl2NO5 5 14.9 8.8 C C P 15+50 2+3 Responses: OV-101: HX16/NI4 bifenthrin C23H22ClF3O2 4.9 3.8 4.5 V C - 6+15 2 Responses: OV-101: NI8 OV-17: HX5/HX(WB)20 binapacryl C15H18N2O6 2.19 4.2 2.38 C P P 15 - Responses: OV-101: NI(WB)1 OV-17: NI22/NP(WB)100 bis(2-ethylhexyl) phthalate C24H38O4 6.4 4.5 6.1 - C C 15+50 - Responses: OV-101: NI(V)200 bis(trichloromethyl)disulfide C2Cl6S2 0.19 - - - R - 6 - Responses: bitertanol* C20H23N3O2 9.4 - 11.8 C - - - - 9.7 - 12.5 Responses: OV-17: NP(WB)200 bromacil C9H13BrN2O2 0.8 4.8 1.36 C NR NR 6-15-50 1-2-3 Responses: OV-101: HN(WB)2/NI(WB)2/NP(WB)17 OV-17: HN(WB)1/HX(WB)8/NI(WB)6/NP(WB)5 OV-225: NI(WB)12 bromacil methyl ether C10H16BrN2O2 0.8 2.1 - - - - - - Responses: OV-101: HN(WB)1.2/HX(WB)90/NI(WB)1.5/NP(WB)10 OV-225: NI(WB)3.8 bromofenoxim methyl ether C14H9Br2O6N3 0.3 - - - - - - - Responses: OV-101: HN(WB)6/NI1 bromophos C8H8BrCl2O3PS 1.11 1.29 1.16 C C C 6 - Responses: OV-101: FP3/NI(WB)1/TI3 OV-17: FP3/NI2 OV-225: NI6 bromophos-ethyl C10H12BrCl2O3PS 1.51 1.42 1.45 C C P 6 - Responses: OV-101: FP3/NI3/TI4 OV-17: FP(WB)0.3 bromopropylate C17H16Br2O3 4.4 6.5 - C C # C # 15+50 1-2-3 Responses: OV-101: TR12

a Appendix l: PESTDATA Chemicals in Order by Chemical Name(continued) Molecular RRT/c Rrt/c rrt/c Formula OV-101 ov-225 Ov-17 303 304 Ethers CH Cl, ioxynil butyrate CllH9Br2NO2 15+50 Responses: OV-101: NIO.5/NP75 o bror C8H5BR2ON Responses: OV-101: N10. 4 CI5HI7Br2NO2 3.14 15+50 Responses: OV-101: N4/NP40 乙2< BTS 27271-HCI CIoH14N2HCI BTS27919 C9HlINO bufencarbi CIsHI9NO2 Bulan Cl6H13C12NO2 3.06 7.5 C 2 Responses: OV-101: NI(WB)I OV-17: NI OV-225: NI6 CIsH24N4S03 2.6 Responses: OV-101: FS(WB)20/NI(WB)8 OV-17: NP(WB)300 butachlor Cl7H26CINO2 173 Responses: OV-101: HX9 OV-17: HX9 OV-225: NIl4 butralin C14H2IN304 22 0.93 6+15+50 Responses: OV-101: NI7/NP3 OV-17: NI6/NP15 OV-225: NI8 butyl benzyl phthalate CI9H2004 4.5 15+50 OV-101: NIS5 CllH23NOS butylisodecyl phthalate C22H34O4 0.82 CIoH2302PS2 27 C 6-15501-23 Responses: OV-101: FP(WB)0.5 OV-17: FP(WB)0. 4/NI(WB)12/NP(WB)0.5 OV-225: FP(WB)I T captafol CIOH9CI4NO2S OV-101: NIS OV-17: NI5

Pesticide Analytical Manual Vol. I APPENDIX I Form FDA 2905a (6/92) Transmittal No. 2000-1 (10/1999) Molecular RRT/c RRT/c RRT/c Name Formula OV-101 OV-225 OV-17 302 303 304 Ethers CH2Cl2 Appendix I–15 Appendix I: PESTDATA Chemicals in Order by Chemical Name (continued) Recoveries bromoxynil butyrate C11H9Br2NO2 0.78 - - - V - 15+50 2 Responses: OV-101: NI0.5/NP7.5 bromoxynil methyl ether C8H5BR2ON 0.3 - - - - - - - Responses: OV-101: NI0.4 bromoxynil octanoate C15H17Br2NO2 3.14 - - - V # - 15+50 2 Responses: OV-101: NI4/NP40 BTS 27271-HCl C10H14N2•HCl - - - - - - - - Responses: BTS 27919 C9H11NO - - - C - - - - Responses: bufencarb* C13H19NO2 - - - - - - - - - -- - -- - -- - -- Responses: Bulan C16H15Cl2NO2 3.06 7.5 4.4 C P P 15 2 Responses: OV-101: NI(WB)1 OV-17: NI5 OV-225: NI6 bupirimate C13H24N4SO3 2 3.7 2.6 C - - - - Responses: OV-101: FS(WB)20/NI(WB)8 OV-17: NP(WB)300 butachlor C17H26ClNO2 1.73 1.83 1.46 C C - 50 - Responses: OV-101: HX9 OV-17: HX9 OV-225: NI14 butralin C14H21N3O4 1.15 1.22 0.93 V C - 6+15+50 - Responses: OV-101: NI7/NP3 OV-17: NI6/NP15 OV-225: NI8 butyl benzyl phthalate C19H20O4 3.06 5.1 4.5 - C P 15+50 - Responses: OV-101: NI35 butylate C11H23NOS 0.22 - - - - - - - Responses: butylisodecyl phthalate C22H34O4 - - 0.82 - - - - - Responses: cadusafos C10H23O2PS2 0.37 0.27 0.29 C NR NR 6-15-50 1-2-3 Responses: OV-101: FP(WB)0.5 OV-17: FP(WB)0.4/NI(WB)12/NP(WB)0.5 OV-225: FP(WB)1 captafol C10H9Cl4NO2S 3.11 - 5.4 C P - 50 3 Responses: OV-101: NI3 OV-17: NI5