Preface and Acknowledgments questions,and key words or phrases are in bold type -a text to help students focus their studies.In this third edition arily for aduate students majoring in-food the middle section of the text has been rearranged into ur dying the analysis of foods.How a gr oup of chapters on compositional analysis and one of the rties and characterization.Hopefully tha t the book is also a valu- nent an im s in the fo try who either do ana with ana this text in whatever order is most suitable for their the the In preparing this third edition the Instituteof b ency e ists side red ent with ality ant to wen food analy conden into n sep the behi P ana aration and characteri cha sociate ith chapters (e.g.government regulations).(4)Change approp e when pr on enzym pro and (3 chapter analysis laboratory. able instr and objectives first new m ents Regrettably,in an effort to make the book a more am third- m manageable size and cost,especially for students,two oe a par of this pro excellent chapters of advanced techniques from the Many authors have drawn on the tea second edition (i.e.,magnetic resonance and analysis ing students and/or experie with analyses t of food emulsions)are not included in the third edi give chapters the approprat conten tion.Readers who need that information are referred to ease of use I also want to thank the pe those chapters in the second edition and also to detailed from the food ndustry who help the books on those techniques.Also,the requests by some in the food analysis courses teach each year, a spe users of this book to add chapters on other topics(e.g. cial project I assign related to quality ass Thes HACCP,sensory evaluation)were considered carefully. However,restrictions on size and cost of the textbook, methods to include in this text. k the and the availability of other resources on these topics, authors of articles and books,and well as the publish have prevented their inclusion in this book. ers and industrial companies,for their permission to As stated for the first and second editions, the reproduce materials used here.I very much apprecate chapters in this textbook are not intended as detailed the valuable suggestions and contribution of new study references,but as general introductions to the top questions for this 3rd edition made by dr lloyd Met ics and the techniques.Course instructors may wish zger of the University of Minnesota.Special thanks is to provide more details on a particular topic to stu- extended to erin addison.Susan axel Bedsaul.loanne dents.Chapters focus on principles and applications of DeRoeck.Wilfredo Dominguez.Christina Kokini.and ven are meant to help explain Cynthia Machado at Purdue University for their assis- the principles and give some examples,but are not tance in word processing,editing,and checking details meant to be presented in the detail adequate to actually in the preparation of this book. specific analysis.As in the first and se S Suzanne nielsen
List of Abbreviations AACC ne can Association of Cereal CIE ission Internationale d'Eclairage em CLND A点 2. scopinc-6 critical micell 26 oxygen den dichloroqu onechloroinmide ariatior ultural Mar on spectroscopy ting Service 1-aniline e sulfonic acid direct current D degree of esterification Chemists EA dielectric analysis American Oil Chemists'Society DEAT dielectric thermal analysis active oxygen method DFE dietary folate quivalent atmospheric pressure chemical DHHS Department of Health and Human ionization Services APHA American Public Health Association DMD D-malate dehydrogenase APPI atmospheric pressure photo-ionization DMSC dimethyl sulfoxide ASE accelerated solvent extraction DMTA dynamic mechanical thermal analysis ASTM American Society for Testing Materials DNFB 1-fluoto-24-dinitrobenzene American Type Culture Collection DNP diitrophenvl ATF Bureau of Alcohol,Tobacco,Firearms DON deoxynivalenol and Explosives DP degree of polymerization ATP adenosine-5'-triphosphate DRV Daily reference value ATR attenuated total reflectance DSC differential scanning calorimetry ATR-FTIR attenuated total reflection-Fourier DSHEA Dietary Supplement Health and transform infrared Education act BAW base and acid washed DTA differential thermal analysis BCA bicinchoninic acid DTNB 5,5-thiobis-2-nitrobenzoic acid BCR Community Bureau of Reference DTR differential thermal rheometry B Baume modulus DV daily value HA butylated hydroxyanisole dwb dry weight basis BH butylated hydroxytoluene EAAI essential aminu acid index OD biochemical oxygen demand EBT eriochrome black T BSA bovine serum albumin ECD BSDA EDS Bacillus thuringiensis EDTA nediaminetetr CAST calf antibiotic and sulfa test EEc ean Economic Cor nity CCD charg -coupled device Cente ers for Disease Control EIE ELCD CFIA tivity detector adian Fo on Agency ELISA of Fe EPA M tal Protec ring Practices cal ionizati equiva relative humidit el CID on device ctieeptaxdntertace
List of Abprevations FAME fatty acid methyl esters IDK insect damaged kernels FAO/WHO Food and Agricultural Organization/ immunoglobulin E World Health Organization immunoglobulin G FAS indiu -gainum-ars FDAMA nd Drg ted pest m men FD&O IRMM Institute for Reference Materials and Measurements free fatty acid internal standard FID Bame ionization detector FIFRA Federal Insecticide,Fungicide,and ectrod Rodenti e Ao al Organization fo FNB/NAS Board of the m 、A JUPAC mational Union of Pure and Applied ection Ac Chemistry Food Safety and Inspection Service JECFA Joint FAO/WHO Expert Committce on Fourier transform Federal Trade Commission Fourier transform- n cyclotrons er reagen orm er rea and Trade angle laser light scattering AED h atomic emission liquid chromatography LC-MS liquid chromatography-mass GC-FTIR gas chromatography-Fourier transfurn infrared Lateral flow strip MS gas ch atography-mass spectrometry s laboratory inform ation managemen GIPSA ers an kyard trix-as nh timof-flight GMA y manufacturers of america MCL maximum contaminant level CMO MDCSTM modulated differential scanning GMP calorimeter GOPOD glucose oxidase/peroxidase milliequivalents gel-permeation chroma methy ocyanate pnos nated MRMs mu sidu ear T the MS ructose syrun MS/MS tandem MS HK MsA multiple stages of mass spectrometry high performance liquid MW molecular weight chromatography m/2 mass-to-charge ratic HPLC-MS high performance liquid HPTLC gh per sP NADP graphy NCWM National Conference on Weights and Measures ICP-AES nductively coupled plasma-atomic NEDM non fat dry milk emission spectroscopy NIR near-infrared ICTA ration for NIST National Institute of Standards and Thermal Analysis ID nner diamete NLEA ng and Education Ac
List of x猫 NMES National marine fisheries service standard deviation NMR nuclear magnetic resonance SDS sodium dodecyl sulfate NOAA National Oceanic and Atmospheric SDS-PAGE sodium dodecyl sulfate-polyacrylamide Administration gel electrophoresi NPD nitrogen phosphorus detector or error of the mear chromatography h P on Progra of th orga solid fat cor OD outer diamete SFC supercritical-fluid chromatography ODS octadecylsilyl SFE supercritical fluid extraction OES optical emission spectroscopy SFE-GO supercritical fluid extraction-gas OPA o-phthalaldehyd tography SIM ed ion m ring PACE l- PAM solid/liquid PAM II Pesticide Analytical Manual,Volume Il solids-not-fat polychlorinated biphenyls SPE solid-phase extraction PCR principal components regression SPME solid-phase microextraction polymerase hilit rimetry 11g TBA thiobarbituric acid polyether ether ketone TBARS TBa roactive substances PER protein efficiency ratio TCD thermal conductivity detector isoelectric point quivalents PID photoionization detector TEMED partial GA tric analysi PM hin 1 TMA hern Purchase Product Description TMCS trimethyichlorusilane parts per million TMS trimethylsilyl parts per trillion TNBS trinitrobenzenesulphonic acid PteC pteroylglutamate total organic carbon PTFE TOF analysis ypyrro RA TS-MS -mass spectrometry RAC raw agricultural commodity TSP RCS rapid scan correlation TSS total soluble solids RDI Reference Daily Intake TSUSA Tariff Schedules of the United States of R relative mobility tate RI ed. reen US RDA nmended Dietary RIA ROS. id One Step assay UV ultraviolet RPAR Rebuttable Presumption Against UV-Vis ultraviolet-visible Registration Vis visible RVA RapidViscoAnalyser volatile organic compounds revolutior s per minut weigh audi Arabian Standar Organization wet weight basis
part General Intormation 1