皖西学浣WEST ANHUIUNIVERSITY化学工程与工艺专业《化工专业实验》指导书材料与化工学院一化工教研室编制2012年5月
１ 化学工程与工艺专业 《化工专业实验》指导书 实验指导书 材料与化工学院—化工教研室 编制 2012 年 5 月
目录实验一串联流动反应器停留时间分布的测定、实验目的二、实验原理·三、实验装置四、实验步骤·五、数据处理六、思考题·实验二固-膜分离实验2一、实验目的1. 2二、基本原理·12三、实验装置与流程4四、实验步骤5实验三管式反应器流动特性测定实验1 7一，实验目的1.7二、实验原理及要点1.7三、装置与流程19四、实验准备工作20五、实验操作指导20六、数据处理·21七、实验报告要求23实验四三组分体系液-液平衡数据测定24实验目的24实验原理·242
２ 目 录 实验一 串联流动反应器停留时间分布的测定············································７ 一、实验目的··················································································································７ 二、实验原理··················································································································７ 三、实验装置··················································································································８ 四、实验步骤··················································································································９ 五、数据处理··················································································································９ 六、思考题··················································································································１１ 实验二 固-膜分离实验 ······································································１２ 一、实验目的···············································································································１２ 二、基本原理···············································································································１２ 三、 实验装置与流程···································································································１４ 四、实验步骤···············································································································１５ 实验三 管式反应器流动特性测定实验··················································１７ 一．实验目的···············································································································１７ 二、实验原理及要点 ····································································································１７ 三、装置与流程···········································································································１９ 四、实验准备工作········································································································２０ 五、实验操作指导········································································································２０ 六、数据处理···············································································································２１ 七、实验报告要求········································································································２３ 实验四 三组分体系液-液平衡数据测定················································２４ 一、 实验目的·············································································································２４ 二、 实验原理·············································································································２４
三、实验仪器及试料2 4四、操作步骤25五、实验记录及数据处理26六、实验报告·27附录·.28实验五筛板塔精馏过程实验2 9一，实验目的·29二.基本原理2.9三。 实验装置和流程33四。实验步骤与注意事项....35五，实验报告36六．思考题36实验六乙苯脱氢制备苯乙烯37一、实验目的37二、实验原理·37三、实验装置及流程·38四、实验准备物料及仪器3 9五、实验步骤及方法39六。数据记录与处理·4.0七、实验结果与讨论1实验七液-液转盘萃取4 5实验目的45二、基本原理45三、.48实验装置与流程四、实验步骤483
３ 三、 实验仪器及试料···································································································２４ 四、 操作步骤·············································································································２５ 五、 实验记录及数据处理····························································································２６ 六、 实验报告·············································································································２７ 附录····························································································································２８ 实验五 筛板塔精馏过程实验 ······························································２９ 一．实验目的···············································································································２９ 二．基本原理···············································································································２９ 三. 实验装置和流程 ····································································································３３ 四．实验步骤与注意事项······························································································３５ 五．实验报告···············································································································３６ 六．思考题··················································································································３６ 实验六 乙苯脱氢制备苯乙烯 ······························································３７ 一、实验目的···············································································································３７ 二、实验原理···············································································································３７ 三、实验装置及流程 ····································································································３８ 四、实验准备物料及仪器······························································································３９ 五、实验步骤及方法 ····································································································３９ 六．数据记录与处理 ····································································································４０ 七、实验结果与讨论 ····································································································４１ 实验七 液-液转盘萃取 ······································································４５ 一、 实验目的···········································································································４５ 二、基本原理···············································································································４５ 三、 实验装置与流程·································································································４８ 四、 实验步骤·············································································································４８
五、实验报告4 9六、思考题50实验八填料塔间歇精馏实验5实验目的51二、基本原理·51三、技术指标与配置51四、操作方法5 1五、故障处理53附录:53实验九果胶的提取及性能测定5 555一、实验目的·55二、实验原理·三、实验药品、仪器、装置5555四、操作步骤·56五、注意事项·六、实验现象及结论记录表56七、问题与思考56实验十丙烯酸酯乳液胶粘剂的制备57、实验目的·57二、实验原理·57三、仪器试剂58四、实验操作58五、注意事项58六、胶接试验59七、思考题594
４ 五、实验报告···············································································································４９ 六、思考题··················································································································５０ 实验八 填料塔间歇精馏实验 ······························································５１ 一、 实验目的···········································································································５１ 二、基本原理···············································································································５１ 三、 技术指标与配置···································································································５１ 四、 操作方法·············································································································５１ 五、 故障处理·············································································································５３ 附录····························································································································５３ 实验九 果胶的提取及性能测定··························································５５ 一、实验目的···············································································································５５ 二、实验原理···············································································································５５ 三、实验药品、仪器、装置 ··························································································５５ 四、操作步骤···············································································································５５ 五、注意事项···············································································································５６ 六、实验现象及结论记录表 ··························································································５６ 七、问题与思考···········································································································５６ 实验十 丙烯酸酯乳液胶粘剂的制备 ···················································５７ 一、实验目的···············································································································５７ 二、实验原理···············································································································５７ 三、仪器试剂···············································································································５８ 四、实验操作···············································································································５８ 五、注意事项···············································································································５８ 六、胶接试验···············································································································５９ 七、思考题··················································································································５９
实验十一6 0防晒膏的配制一、实验目的·60-二、实验原理60三、仪器及试剂·60四、实验操作60五、思考题61实验十二抗氧剂双酚A的合成6 2实验目的·62二实验原理.62三主要仪器和药品63四实验步骤·63五注意事项6364实验十三食品抗氧剂没食子酸丙酯的合成一、实验目的·64二、实验原理·64三、仪器试剂·65四、实验操作6 5五、思考题656 6实验十四餐具洗涤剂的制备一、实验目的66二、产品特性与用途66三、实验原理66四、主要仪器与药品6.767五、实验内容与操作步骤68六、实验记录与数据处理5
５ 实验十一 防晒膏的配制 ···································································６０ 一、实验目的···············································································································６０ 二、实验原理···············································································································６０ 三、仪器及试剂···········································································································６０ 四、实验操作···············································································································６０ 五、思考题··················································································································６１ 实验十二 抗氧剂双酚 A的合成···························································６２ 一 实验目的···············································································································６２ 二 实验原理···············································································································６２ 三 主要仪器和药品 ····································································································６３ 四 实验步骤···············································································································６３ 五 注意事项···············································································································６３ 实验十三 食品抗氧剂没食子酸丙酯的合成 ···········································６４ 一、实验目的···············································································································６４ 二、实验原理···············································································································６４ 三、仪器试剂···············································································································６５ 四、实验操作···············································································································６５ 五、思考题··················································································································６５ 实验十四 餐具洗涤剂的制备 ······························································６６ 一、实验目的···············································································································６６ 二、产品特性与用途 ····································································································６６ 三、实验原理···············································································································６６ 四、主要仪器与药品 ····································································································６７ 五、实验内容与操作步骤······························································································６７ 六、实验记录与数据处理······························································································６８