MECHANICALMAGNETRON/DCSTIRRERPOWERSOURCEREACTORPROGRAMMABLEMICROWAVETHERMOSTATTEMPERATURECONTROLLERUNIT
Microwave irradiation raises the temperature of thewhole volume simultaneously (i.e. bulk heating)bOilbathMicrowave460500440450420400400380360350340300320
Microwave irradiation raises the temperature of the whole volume simultaneously (i.e. bulk heating)
Reviewof Microwavemethod>To use microwave heating in solidstatesynthesis at least one component of the reactionmixture must absorb microwave radiationwith>Advantage:lessproblemscracking,decreases reaction time>Shortcoming: does not solve the problem ofchemical inhomogeneity and temperatures in thereaction are high
Review of Microwave method To use microwave heating in solid state synthesis at least one component of the reaction mixture must absorb microwave radiation Advantage: less problems with cracking, decreases reaction time Shortcoming: does not solve the problem of chemical inhomogeneity and temperatures in the reaction are high